| Alloy identity |
The declared alloy grade, nominal composition, balance magnesium, and permitted impurity limits should match the purchase specification. |
Material certificate showing elemental composition for each production lot. |
Optical emission spectroscopy, X-ray fluorescence, or another validated elemental-analysis method. |
Generic “magnesium alloy powder” description without a defined alloy designation or impurity limits. |
| Particle-size distribution |
The D10, D50, D90 range and maximum oversize should be agreed in advance. Common atomized powder specifications may use ranges such as 15–45 µm, 45–90 µm, or 90–150 µm, depending on the application. |
Lot-specific particle-size report, including test dispersion conditions and sample preparation. |
Laser diffraction in accordance with ISO 13320, or sieve analysis for coarser fractions. |
Only a nominal mesh size is supplied; fines and oversize particles are not reported. |
| Particle morphology |
Particles should be predominantly spherical or near-spherical when the powder is intended for powder-bed or other flow-sensitive processes. Satellites, hollow particles, and irregular particles should be controlled. |
Representative scanning electron microscope images and a morphology assessment. |
Scanning electron microscopy with images from more than one field of view. |
Images are unavailable, heavily enlarged without scale information, or show excessive agglomeration. |
| Oxygen and surface oxidation |
An oxygen limit must be defined for the specific alloy and process. A frequently used screening target is ≤0.30 wt%, but the applicable value must be validated for the end use. |
Lot-specific oxygen result, analytical uncertainty, and test method. |
Inert-gas fusion or another validated oxygen-analysis method, such as ASTM E1019 where applicable. |
Oxygen is reported only as “low” or is measured from a pooled sample without lot identification. |
| Moisture and volatile content |
Moisture should be controlled to the application specification; for many dry powder processes, a target of ≤0.05 wt% is used as a screening value. |
Moisture result, sampling date, packaging condition, and storage history. |
Validated loss-on-drying, Karl Fischer, or another suitable moisture method. |
Wet containers, damaged seals, visible clumping, or no moisture result on the certificate of analysis. |
| Apparent density |
The value should be consistent with the agreed particle-size distribution and morphology. A single universal pass/fail value should not be used for every alloy and size fraction. |
Lot-specific apparent-density result and test conditions. |
ISO 3923-1 or an equivalent validated apparent-density method. |
Large unexplained variation between lots or a result without particle-size information. |
| Flowability |
Flow performance should be evaluated against the intended equipment. Hall flow time, when measurable, should be reported with the tested mass and funnel specification. |
Flow-rate result, test temperature, humidity, and sample conditioning procedure. |
ISO 4490 or another process-appropriate powder-flow method. |
Supplier claims “free flowing” without a numerical result or test conditions. |
| Contamination control |
Foreign metal, ceramic, oil, and cross-alloy contamination should be controlled by dedicated equipment or validated cleaning procedures. |
Contamination-control plan, equipment-cleaning records, and nonconformance history. |
Visual inspection, microscopy, magnetic separation checks where relevant, and chemical analysis. |
Shared production lines with no documented cleaning validation or unexplained foreign particles. |
| Packaging and inert atmosphere |
Powder should be sealed in moisture-resistant packaging, normally under a dry inert atmosphere when required by the risk assessment and product specification. |
Packaging specification, fill date, seal inspection, and recommended storage conditions. |
Incoming-package inspection and verification of seal integrity and storage humidity. |
Unsealed bags, excessive headspace air, corrosion, condensation, or missing storage instructions. |
| Safety Data Sheet and GHS classification |
A current, product-specific SDS should identify combustible-dust, flammability, reactivity, first-aid, handling, storage, and disposal hazards. |
Current SDS in the destination-country language and revision-controlled format. |
Review against the applicable GHS implementation and local workplace-safety regulations. |
SDS is generic, outdated, missing dust-hazard information, or inconsistent with the powder's particle size. |
| Fire and explosion controls |
The supplier should provide controls for ignition sources, dust accumulation, static electricity, ventilation, and emergency response. Magnesium powder fires require a suitable Class D extinguishing agent; water and carbon dioxide may be hazardous for burning magnesium. |
Written handling guidance, fire-response procedure, dust-explosion assessment, and employee training records. |
Site safety review and confirmation with the facility's qualified fire-safety professional. |
Recommendation to use water or carbon dioxide without qualification, or no combustible-dust controls. |
| Transport classification |
The applicable dangerous-goods classification, packing group, labeling, and transport mode must be determined from the actual powder characteristics and current SDS. |
Transport declaration, UN identification where applicable, packaging instruction, and carrier requirements. |
Review under the applicable ADR, IMDG, IATA, or national transport regulations. |
Supplier cannot provide transport information or uses the same classification for every particle-size fraction. |
| Lot and batch traceability |
Every container should be linked to the alloy melt or raw-material lot, atomization batch, production date, test results, packaging date, and shipment record. |
Traceability map, lot numbering procedure, production records, and retain-sample policy. |
Select a shipment lot and verify backward and forward traceability through the supplier's records. |
Container labels do not match the certificate of analysis or the supplier cannot identify the original melt. |
| Certificate of analysis |
The certificate should be lot-specific and include chemical composition, particle-size distribution, oxygen, moisture, density, flowability, and release status where applicable. |
Signed or electronically controlled certificate with test dates, methods, units, limits, and actual results. |
Compare the certificate with the purchase order and independently test a pre-production sample. |
A certificate shows only typical values, not actual lot results. |
| Quality-management system |
A documented quality system with controlled procedures, calibration, nonconformance management, corrective action, and change control should be in place. |
Quality-system certificate or audit report, calibration records, corrective-action examples, and internal-release procedure. |
Supplier questionnaire, remote audit, or on-site audit based on risk. |
No documented change-notification process or repeated unexplained lot variation. |
| Change notification |
The supplier should notify the buyer before changes to alloy feedstock, atomization parameters, sieving, equipment, packaging, test methods, or production location. |
Formal change-control procedure and agreed notification period. |
Review historical changes and confirm that affected lots were identified. |
Unannounced process changes or a statement that all changes are “equivalent” without supporting data. |
| Sampling and approval process |
Approve the supplier using representative samples from multiple lots rather than relying on one sample or a catalog specification. |
Pre-production samples, sampling plan, retain samples, and customer complaint procedure. |
Test at least three non-consecutive lots when feasible and compare results with process capability. |
Supplier refuses independent testing or provides only a hand-selected demonstration sample. |